Removal of Pb(II) Metal Ions from Aqueous Solutions Using Chitosan-Vanillin Derivatives of Chelating Polymers

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About the Journal In Memory of Professor Jerzy Radecki Ownership and Management Statement Editorial Office Editorial Board Scope Impact Factor Indexed by Journal Impact Factor contributing items Publication Frequency Revenue Sources & Business Model Contact Subscription

Current issue

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Instructions for Authors Copyright & Licensing Publication Fees

Editorial policies Publication Policy Overview Peer Review Policy Research Ethics and Malpractice Policy Plagiarism Policy Conflict of Interest Policy Open Access Policy Instructions for Reviewers Generative AI and AI-Assisted Technologies Policy Advertising Policy Direct Marketing & Manuscript Solicitation Digital Archiving and Preservation Policy CrossMark, Correction, and Retraction Policy

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ORIGINAL RESEARCH

Removal of Pb(II) Metal Ions from Aqueous Solutions Using Chitosan-Vanillin Derivatives of Chelating Polymers

Fadi Alakhras ¹

,

Hanin Al-Shahrani ¹

,

Eman Al-Abbad ¹

,

Fuad Al-Rimawi ²

,

Noureddine Ouerfelli ¹

1

Department of Chemistry, College of Science, Imam Abdulrahman Bin Faisal University, Dammam, Saudi Arabia

2

Depertment of Chemistry and Chemical Technology, Faculty of Science and Technology, Al-Quds University, Jerusalem, Palestine

Submission date: 2017-12-31

Final revision date: 2018-03-25

Acceptance date: 2018-03-26

Online publication date: 2018-12-12

Publication date: 2019-02-18

Corresponding author

Fadi Alakhras

Imam Abdulrahman Bin Faisal University, P.O.Box: 1982 Dammam 31441 (Al Rayan Dist.), Saudi Arabia, 31441 Dammam, Saudi Arabia

Pol. J. Environ. Stud. 2019;28(3):1523-1534

DOI: https://doi.org/10.15244/pjoes/89545

KEYWORDS

chitosan-vanillin Schiff base

chelating polymers

wastewater treatment

TOPICS

ABSTRACT

Our study investigates the removal of Pb(II) ions found in aqueous solutions using chitosan-vanillin polymeric material. The effects of pH, agitation time, adsorbent mass, and initial amount of studied ion on the chelation process have been carried out using batch experiments. The quantity of residual ions has been estimated via atomic absorption spectrometry. The polymers are characterized using infrared spectroscopy, TGA, SEM, and BET surface area.
The highest removal of Pb(II) ions achieved by polymers I and II was at pH 6. The Langmuir isotherm worked as the greatest explanation for the experimental outcome with highest chelation capability equal to 23.3 mg g^-1 for polymer I and 66.23 mg g^-1 for polymer II. Kinetic studies revealed that chemisorption was the rate-determining step, whereas the uptake was natural and endothermic.

CONFLICT OF INTEREST

The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

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