ORIGINAL RESEARCH
Physicochemical Properties of Ethiopian
Orange (Citrus sinensis) Peels
and Extracted Pectin by Varieties
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1
Department of Food Engineering, Kombolcha Institute of Technology, Wollo University, Ethiopia
2
Department of Chemistry, Wollo University, Ethiopia
3
UGA Cooperative Extension, University of Georgia, Athens, GA 30602, USA
These authors had equal contribution to this work
Submission date: 2024-01-10
Final revision date: 2024-02-23
Acceptance date: 2024-06-12
Online publication date: 2024-09-13
Publication date: 2025-05-09
Corresponding author
Abebe Teshome Ayele
Department of Food Engineering, Kombolcha Institute of Technology, Wollo University, Ethiopia
Pol. J. Environ. Stud. 2025;34(4):4009-4016
KEYWORDS
TOPICS
ABSTRACT
The physicochemical properties of Ethiopian orange (Citrus sinensis) peels and their extracted
pectin by varieties were investigated. Specifically, orange (peel) varieties included Valencia, Mandarin,
and Gunda Gundo, and their extracted pectin was physicochemically characterized in terms of yield,
moisture, ash, viscosity, acetyl, equivalent weight, methoxyl, degree of esterification, and anhydrouronic
acid aspects. In many instances, the physicochemical properties of extracted pectin differed significantly
(p<0.05). For instance, the extracted pectin from the Mandarin peel variety showed greater yield,
viscosity, equivalent weight, methoxyl, anhydrouronic acid, and degree of esterification, but less
acetyl, moisture, pH, and ash. Contrarily, the extracted pectin from Valencia showed greater acetyl
concentration, moisture, and ash content but less yield, viscosity, equivalent weight, anhydrouronic
acid, and esterification. Feasibly, the Mandarin variety appears to be a rich pectin resource with high
promise as a significant raw material for the food processing industry.
CONFLICT OF INTEREST
The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.
REFERENCES (29)
1.
PATHAK D., AGRAWAL P., EFROS A.A., DARRELL T. Curiosity-driven exploration by self-supervised prediction. Proceedings of Machine Learning Research, 70, 2778, 2017.
https://doi.org/10.1109/CVPRW.....
2.
MITREA L., CALINOIU L.F., TELEKY B.E., SZABO K., MARTĂU A.G., NEMES S.A., PLAMADA D., PASCUTA M.S., BARTA G., VARVARA R.A., VODNAR D.C. Fruit and vegetable wastes for biobased chemicals, In: Mandavgane S.A., Chakravarty I., and Jaiswal A.K. (Eds), Fruit and Vegetable Waste Utilization and Sustainability, Elsevier Inc.: Cambridge MA-USA, 43, 2023.
https://doi.org/10.1016/B978-0....
3.
ARSHAD Y.M., RASHID A., GUL H., AHMAD A.S., JABBAR F. Optimization of acid-assisted extraction of pectin from banana (Musa acuminata) peels by central composite design. Global NEST Journal, 24, 752, 2022.
4.
KARIM R., NAHAR K., ZOHORA F.T., MONARUL ISLAM MD., BHUIYAN R.H., SARWAR J.M., AFTAB A.S.MD. Pectin from lemon and mango peel: Extraction, characterisation and application in biodegradable film. Carbohydrate Polymer Technologies and Applications, 4, 100258, 2022.
https://doi.org/10.1016/j.carp....
5.
EL FIHRY N., EL MABROUK K., EECKHOUT M., SCHOLS H.A., FILALI-ZEGZOUTI Y., HAJJAJ H. Physicochemical and functional characterization of pectin extracted from Moroccan citrus peels. LWT, 162, 113508, 2022.
https://doi.org/10.1016/j.lwt.....
6.
SPINEI M., OROIAN M. The influence of extraction conditions on the yield and physico-chemical parameters of pectin from grape pomace. Polymers, 14 (7), 1378, 2022.
https://doi.org/10.3390/polym1... PMid:35406252 PMCid:PMC9002691.
7.
LACHOS-PEREZ D., BASEGGIO A.M., TORRES-MAYANGA P.C., ÁVILA P.A., TOMPSETT G.A., MAROSTICA M., GOLDBECK R., TIMKO M.T., ROSTAGNO M., MARTINEZ J., FORSTER-CARNEIRO T. Sequential subcritical water process applied to orange peel for the recovery flavanones and sugars. The Journal of Supercritical Fluids, 160, 104789, 2020.
https://doi.org/10.1016/j.supf....
8.
SHIN Y., CHANE A., JUNG M., LEE Y. Recent advances in understanding the roles of pectin as an active participant in plant signaling networks. Plants, 10 (8), 1712, 2021.
https://doi.org/10.3390/plants... PMid:34451757 PMCid:PMC8399534.
9.
FREITAS C.M.P., COIMBRA J.S.R., SOUZA V.G.L., SOUSA R.C.S. Structure and applications of pectin in food, biomedical, and pharmaceutical industry: A review. Coatings, 11 (8), 922, 2021.
https://doi.org/10.3390/coatin....
10.
KHAMSUCHARIT P., LAOHAPHATANALERT K., GAVINLERTVATANA P., SRITOTH K., SANGSEETHONG K. Characterization of pectin extracted from banana peels of different varieties. Food Science and Biotechnology, 27, 623, 2018.
https://doi.org/10.1007/s10068... PMid:30263788 PMCid:PMC6049672.
11.
TESHOME A., ADMASSU H., MOHAMMED F. Evaluation of Selected Locally Grown Sweet Potato (Ipomoea batatas) Varietal Suitability on Fried Chips Quality. Journal of Culinary Science & Technology (in-press), 1, 2022.
https://doi.org/10.1080/154280....
12.
SIKDER M.B.H., AHMED S. Extraction, characterization and application of three varieties of Citrus limon L. pectin in jelly product. Food and Applied Bioscience Journal, 7 (1), 31, 2019.
13.
KAREEM A.H., NAJI E.Z. Study of the Chemical Properties of Pectin Extracted from Residues of Some Plant Sources. Annals of Biology, 38, 252, 2022.
14.
OWOEYE T., AKINLABU D.K., AJAYI O.O., AFOLALU S.A., POPOOLA J.O., AJANI O.O. Phytochemical constituents and proximate analysis of dry pineapple peels. IOP Conference Series: Earth and Environmental Science, 993, 012027, 2022.
https://doi.org/10.1088/1755-1....
15.
TRAN H.N., YOU S.-J., CHAO H.-P. Effect of pyrolysis temperatures and times on the adsorption of cadmium onto orange peel derived biochar. Waste Management & Research, 34 (2), 129, 2016.
https://doi.org/10.1177/073424... PMid:26608900.
16.
M'HIRI N., IOANNOU I., GHOUL M., MIHOUBI BOUDHRIOUA N. Proximate chemical composition of orange peel and variation of phenols and antioxidant activity during convective air drying. Journal of New Sciences, 82 (9), 881, 2015.
17.
NIDHINA K., ABRAHAM B., FONTES-CANDIA C., MARTÍNEZ-ABAD A., MARTÍNEZ-SANZ M., NISHA P., LOPEZ-RUBIO A. Physicochemical and functional properties of pectin extracted from the edible portions of jackfruit at different stages of maturity. Journal of the Science of Food and Agriculture, 103 (6), 3194, 2023.
https://doi.org/10.1002/jsfa.1... PMid:36534030.
18.
AYALA J.R., MONTERO G., CORONADO M.A., GARCIA C., CURIEL-ALVAREZ M.A., LEÓN J.A., SAGASTE C.A., MONTES D.G. Characterization of orange peel waste and valorization to obtain reducing sugars. Molecules, 26 (5), 1348, 2021.
https://doi.org/10.3390/molecu... PMid:33802601 PMCid:PMC7961523.
19.
LEKHULENI I.L.G., KGATLA T.E., MASHU M.E. Physicochemical properties of South African prickly pear fruit and peel: Extraction and characterisation of pectin from the peel. Open Agriculture, 6 (1), 178, 2021.
https://doi.org/10.1515/opag-2....
20.
PATHAK P.D., MANDAVGANE S.A., KULKARNI B.D. Fruit peel waste: characterization and its potential uses. Current Science, 113 (3), 444, 2017.
https://doi.org/10.18520/cs/v1....
21.
RAHMAN MD.S., KHAN S.S., WADUD AHMED MD., ENTADUZZAMAN JONY MD., CHANDRA AS P., BURHAN UDDIN MD. Extraction of pectin from Elephant Apple and Pomelo fruit peels: Valorization of fruit waste towards circular economy. Food Chemistry Advances, 3, 100544, 2023.
https://doi.org/10.1016/j.foch....
22.
WANG W., MA X., XU Y., CAO Y., JIANG Z., DING T., YE X., LIU D. Ultrasound-assisted heating extraction of pectin from grapefruit peel: Optimization and comparison with the conventional method. Food Chemistry, 178, 106, 2015.
https://doi.org/10.1016/j.food... PMid:25704690.
23.
COLODEL C., VRIESMANN L.C., DE OLIVEIRA PETKOWICZ C.L. Rheological characterization of a pectin extracted from ponkan (Citrus reticulata blanco cv. ponkan) peel. Food Hydrocolloids, 94, 326, 2019.
https://doi.org/10.1016/j.food....
24.
SUSANTI S., LEGOWO A.M., SILVIANA N., ARIFAN F. Comparing the chemical characteristics of pectin isolated from various Indonesian fruit peels. Indonesia Journal of Chemistry, 21 (4), 1057, 2021.
https://doi.org/10.22146/ijc.5....
26.
TWINOMUHWEZI H., GODSWILL A.C., KAHUNDE D. Extraction and characterization of pectin from orange (Citrus sinensis), lemon (Citrus limon) and tangerine (Citrus tangerina). American Journal of Physical Sciences, 1 (1), 17, 2023.
https://doi.org/10.47604/ajps.....
27.
ALTAF U., IMMANUEL G., IFTIKHAR F. Extraction and characterization of pectin derived from papaya (Carica papaya Linn.) peel. International Journal of Science, Engineering and Technology, 3 (4), 970, 2015.
28.
VANITHA T., KHAN M. Role of pectin in food processing and food packaging. In: Masuelli, M. (Ed.), Pectins: extraction, purification, characterization and applications. Intechopen, 6, 78880, 2020.
https://doi.org/10.5772/intech....
29.
RODSAMRAN P., SOTHORNVIT R. Preparation and characterization of pectin fraction from pineapple peel as a natural plasticizer and material for biopolymer film. Food and Bioproducts Processing, 118, 198, 2019.
https://doi.org/10.1016/j.fbp.....